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Polarity determination of zinc oxide nanorods by defocused convergent-beam electron diffraction
Authors:D. P. Nicholls  R. Vincent  D. Cherns  Y. Sun  M. N. R. Ashfold
Affiliation:1. H.H. Wills Physics Laboratory , University of Bristol , UK david.nicholls@bris.ac.uk;3. H.H. Wills Physics Laboratory , University of Bristol , UK;4. School of Chemistry , University of Bristol , UK
Abstract:The crystal polarity of wurtzite zinc oxide nanorods grown hydrothermally parallel to the c?=?[0001] direction has been determined by convergent-beam electron diffraction using a defocused probe. The method enables a simple comparison of the diffracted intensities in ±0002 reflections across side-on nanorods, demonstrating growth in this case is in the c?=?[0001] direction. The method is shown to be viable for nanorods down to about 11?nm in diameter.
Keywords:
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