HRTEM observation of misfit dislocations at non-faceted Al–Pb interfaces

Al–Pb samples containing 1?at.%?Pb were produced by high-energy ball milling and investigated by high-resolution transmission electron microscopy. The Pb inclusions embedded in an Al matrix exhibit a non-faceted, curved morphology. Dislocations have been found to accommodate the misfit of about 22% at the Al–Pb interfaces. Burgers circuits, drawn around these misfit dislocations, exhibit closing failures of the type a₀ /4〈211〉.     

Effect of severe plastic deformation on the coercivity of Co–Cu alloys

Cast Co–5.6 wt% Cu and Co–13.6 wt% Cu alloys were subjected to severe plastic deformation (SPD) by high-pressure torsion (HPT). The HPT treatment drastically decreases the size of the Co grains (from 20 µm to 100 nm) and the Cu precipitates (from 2 µm to 10 nm). As a result, the coercivity H _c of both the alloys radically increases. The saturation magnetization, M _s, remains almost unchanged. Thus, SPD of the bulk samples opens the way for drastic increase in the coercivity for the Co-based alloys.     

High-temperature nanoindentation behavior of Al/SiC multilayers

Nanoscale Al/SiC composite laminates have unique properties, such as high strength, high toughness, and damage tolerance. In this article, the high-temperature nanoindentation response of Al/SiC nanolaminates is explored from room temperature up to 300°C. Selected nanoindentations were analyzed postmortem using focused ion beam and transmission electron microscopy to ascertain the microstructural changes and the deformation mechanisms operating at high temperature.     

Adorno’s Negative Dialectic: Theme,Point, and Methodological Status

Abstract

This paper provides a criticial interpretation of the theme, point, and methodological status of Adorno’s so‐called negative dialectic. The theme at issue, ‘non‐identity’, comes in several varieties; and the point of Adorno’s dialectic, namely reconciliation, is multifaceted. Exploration of those topics shows that negative dialectic seques into substantive doctrines, including a version of transcendentalism and a claim about deformation. The peculiar methodological status of negative dialectic explains that adumbration. In the appraisive register, my principal contentions include these: Adorno’s transcendentalism makes some sense of the aforementioned deformation claim; and negative dialectic qua method avoids mystery and metaphysical excess.     

A model for 〈c+a〉 dislocation transmission across nano-spaced parallel basal stacking faults in a HCP alloy

We develop a model for recently observed 〈c + a〉 dislocation transmission across nano-spaced parallel basal stacking faults in hexagonal close-packed (HCP) Mg microcrystalline grains. The model theoretically predicts nanospace-dependent yield strength that is in good agreement with experimental data. Additionally, it theoretically predicts activation volume and strain rate sensitivity.     

Influence of strain rate on the orientation dependence of microstructure in nickel single crystals

The deformation microstructures of nickel single crystals (99.945 wt.%) during dynamic plastic deformation and quasi-static compression to a true strain of 0.20 were comparatively investigated. The deformation microstructures are orientation dependent, forming cell structure, slip plane aligned or not slip plane aligned extended boundaries. It is found that the orientation spread decreases, remains unchanged and becomes enhanced when loading along 〈0?0?1〉, 〈0?1?1〉 and 〈1?1?1〉, respectively, as strain rate increases.     

Influence of mode of deformation on microstructural heterogeneities in Ni subjected to large strain deformation

In the present work, the effect of deformation mode (uniaxial compression, rolling and torsion) on the microstructural heterogeneities in a commercial purity Ni is reported. For a given equivalent von Mises strain, samples subjected to torsion have shown higher fraction of high-angle boundaries, kernel average misorientation and recrystallization nuclei when compared to uniaxially compressed and rolled samples. This is attributed to the differences in the slip system activity under different modes of deformation.     

A variant selection mechanism in the deformed and recrystallized β matrix of a metastable β-titanium alloy

ABSTRACT

The variant selection criteria during β to α phase transformations in a metastable β-titanium alloy (Ti-5553) in the presence of deformation are examined. Two distinct metallurgical states in the β matrix, heavily deformed and fully recrystallized, were obtained from a 90% cold-rolled alloy. The deformed and recrystallized samples were subjected to aging heat treatment for a short time to allow the precipitation of an intragranular α phase. Electron backscattered diffraction was used to assess the α crystallographic variant occurrence in the deformed as well as in the recrystallized β grains. A discrete pole figure analysis revealed that a limited number of variants were evolved in the deformed β grains while there was no variant selection in the recrystallized β matrix. The results suggest that activation of {112}<111>_β slip systems determines a strong variant selection in the plastically deformed β matrix.     

Equivalent and effective strains during severe plastic deformation (SPD)

ABSTRACT

This paper considers the characteristics of severe plastic deformation (SPD) to estimate its efficacy and to compare different processing techniques. In contrast to effective strains by von Mises and Hencky, the rotation component of the strain rate is included in the analysis as a mode of deformation, which ranges from simple shear to pure shear. Distortions of material elements during a uniform plane plastic flow are calculated using a kinematic approach. For the fixed deformation mode, the current state is defined by the accumulated shears that are identical to the von Mises effective shear strains. In specific cases of pure shear and simple shear, the accumulated shears match the specific distortions of round or square elements prescribed by Hencky or von Mises approach, respectively. The mode of deformation is important to the structural effects of SPD. In general, two separated characteristics, accumulated shear and the coefficient of deformation mode, are necessary to describe strains during SPD.     

Fragmentation testing for ductile thin films on polymer substrates

Fragmentation testing of thin films on substrates has in the past been mostly performed in situ using optical and scanning electron microscopy. While these techniques work well for brittle materials, they cannot always discern the difference between through-thickness cracks (TTCs) and localized plastic deformation of ductile films. Here, we describe fragmentation testing with atomic force microscopy and present criterion to distinguish TTCs and localized deformation for ductile films.