Amorphization under fracture surface in hydrogen-charged and low- temperature tensile-tested austenitic stainless steel

ABSTRACT

The microstructure just below the fracture surface in hydrogen-charged stable austenitic SUS 316L stainless steel, which was subjected to a low strain rate tensile test at ?70°C, was studied by a combination of the focused-ion-beam method and transmission electron microscopy. An amorphous region with a chemical composition almost identical to that of the polycrystalline region was found under the lath-like structure on the fracture surface, although no deterioration of tensile properties by hydrogen appeared. In the amorphous region, band-like regions with wavy contrasts were observed, which were often accompanied by cracks at the boundaries. The presence of the amorphous region with band-like regions implies that amorphization occurred due to high-density vacancies accompanied by agglomerations of excess vacancies in the hydrogen-charged SUS 316L stainless steel that was tensile-tested at low temperatures.     

Evolution of grain-boundary character distribution during iterative processing of an austenitic stainless steel

The present article deals with the analysis of grain-boundary character distribution (GBCD) and microstructural characteristics after iterative processing of austenitic stainless steel, AISI 316L. The steel was subjected to iterative cold reduction and subsequent annealings. After an initial decrease in the fraction of Σ3 boundaries, the number of these increases in subsequent steps. The results relate the importance of iterative processing and the mechanism of obtaining a higher fraction of Σ3 boundaries.     

Microstructures and tensile properties of 304 steel with dual nanocrystalline and microcrystalline austenite content prepared by aluminothermic reaction casting

The microstructures of 304 stainless steels with different amounts of nanocrystalline and microcrystalline austenite prepared by an aluminothermic reaction casting, without and with annealing at 1073?K for 8?h, have been investigated by X-ray diffraction, an electron probe micro-analyser, a transmission electron microscope and a scanning electron microscope. The steels, both without and with annealing, consisted of different dual nanocrystalline and microcrystalline austenite combinations and a little nanocrystalline δ ferrite, while the average grain size of the nanocrystalline austenite increased from 19 to 26?nm and volume fraction of the microcrystalline austenite increased from 17 to 30% after annealing. The tensile strength of the steel was dramatically increased from 500 to 1000?MPa and the tensile elongation ratio increased from 8 to 12% after annealing. However, the tensile strength was decreased to 600?MPa and the tensile elongation ratio increased from 12 to 22% after an annealing at 1273?K. The combination of dual nanocrystalline and microcrystalline austenite obtained after the annealing at 1073?K results in the best tensile properties.