Deposition-rate dependence of granular size distribution in Cu aggregate on liquid substrate studied by atomic force microscopy

In this article, we report an atomic force microscopy study on the microstructure and the deposition-rate dependence of granular size distribution in copper (Cu) ramified aggregates on a liquid substrate. This study shows that the ramified Cu aggregates are composed of Gaussian size distribution granules, which form immediately after the Cu atoms are deposited. The interesting phenomenon is that the mean diameter Φ_m of the granules exponentially decays and approaches a stable value Φ_c with an increase in the deposition rate f. The granular mean diameter Φ_m slightly changes with the time interval Δt during which the film is kept in the vacuum chamber, owing to the large diffusion coefficient of the Cu granules on the liquid substrates. The experimental behavior strongly depends on the properties of the liquid substrate.     

Quantification of dislocation structures at high resolution by atomic force microscopy of dislocation etch pits

Atomic force microscopy of dislocation etch pit structures is a convenient means of characterising the dislocation structure in etchable materials at high resolution for dislocation spacing extending down to 25 nm . This is demonstrated for single crystals of CaF₂. The local deformation zone generated around nanoindents at ambient temperature and the low-angle boundaries generated in the bulk during uniaxial compression at elevated temperatures are presented as examples.