{111} Glide in Ni3Al at room temperature. In situ observations under weak-beam conditions

Abstract

In situexperiments are performed in Ni₃AL at room temperature. We observe reversible changes of antiphase boundary (APB) planes between {111} and {100}, and movements in {111} planes controlled by the crossing of sessile positions with the APB plane in {111}.     

Derivation of the antiphase-boundary energy of L1 2 long-range-ordered precipitates from measurements of the minimum size of stable dislocation loops

In an alloy that is strengthened by long-range-ordered particles, a matrix dislocation generates an antiphase boundary (APB) when it cuts through such a particle. The specific energy n APB of this APB has been measured for two fcc alloys with spherical coherent L12 ordered particles: an Al-7.5at.%Li-alloy and the commercial Ni-base superalloy Nimonic PE16. Peak-aged specimens have been deformed and Orowan loops searched for using transmission electron microscopy. n APB has been derived from the radii of the smallest dislocation loops which have been left behind around particles. Such an approach had been used previously, for example, by Raynor and Silcock and by Nembach et al . Here an improved evaluation method has been applied; it is based on the results of computer simulations of the equilibrium configurations of dislocation loops.     

Transition from diffusive to ballistic capture related to hydrogen incorporation in amorphous silicon

Three intersection mechanisms with the gliding planes (111)_TB, (001)_TB and (115)_TB respectively have been observed by high-resolution electron microscopy in the type-I twin intersection of gamma-TiAl. It was found that the intersection mechanism that occurred was related to the thickness of the incident twin. The accommodation mechanism on the (111)_TB atomic plane is preferred when the incident twin becomes very thin. The dislocation dissociations of the (111)_TB plane accommodation are the most energetically unfavourable of the dissociations of the three intersection mechanisms; however, the resultant dislocations on the (111)_TB planes are the easiest to propagate away from the intersection area. Accordingly, (111)_TB atomic plane accommodation is considered to be the only mechanism allowing shear transmission under the small local stress of the pile-up of the incident twinning partials.     

The crystallographic structure of λ transition-alumina compared with the periodic antiphase boundary structure of a Ga2O3-rich Mg gallate

One of the high-temperature metastable phases found in the MgGa₂O₄–Ga₂O₃ system is the ε_Mg non-stoichiometric Mg gallate. It has a one-dimensional periodic antiphase boundary (PAPB) structure based on the spinel structure. The APBs are parallel to the {3?1?0} planes and the APB vectors are of the 1/4?1 1 0? type when referred to the spinel structure. This generally leads to the existence of 12 monoclinic twin variants in the studied samples. By comparing the X-ray or electronic diffraction patterns of both phases, it will be shown that the recently discovered?λ?transition-alumina has the same type of structure.     

Dissociation of dislocations in MgAl2O4 spinel deformed at low temperatures

Abstract

When spinel is deformed in compression at 400°C along 〈110〉, the primary slip plane is found to be {111} with cross-slip occurring on a {001} plane. A comparison of weak-beam images of dislocations from both systems indicates that all dislocations which belong to the primary slip plane are dissociated out of the {111} plane independent of the character of the dislocation. It is proposed that deformation occurs by motion of dislocations in their dissociated state and that the partial dislocations actually glide on parallel glide planes. Movement of these dissociated dislocations is then accompanied by a concurrent migration of the stacking fault which takes place by a local shuffling of the cations. A stacking fault energy for conservative dissociation at 400°C on {001} of 530±90mJ m^?2 has been determined from weak-beam images of screw dislocations.     

HREM study of the chemical nature of twin planes in CuAlO2

Abstract

High-resolution electron microscopy has been used to study the atomic structure of twins in the binary oxide CuAlO₂. This compound is an occasional product of the bonding between pre-oxidized copper and alumina; its peculiarity is to exhibit a twinned microstructure, owing to the occurrence of two enantiomorphic right- and left-handed configurations. The microstructural examination at high resolution reveals that twin planes are located on copper basal planes rather than aluminium planes; this result is discussed on the basis of an analysis of the various possible stacking sequences which can reasonably be considered to occur at the twin interfaces.     

Stacking fault and dislocation glide on the basal plane of graphite

Generalized stacking-fault energies for the basal plane of graphite are calculated from first principles for slip along two high-symmetry directions. The rhombohedral fault energy compares well with experiment and the anisotropy in behaviour is consistent with observed dislocation network geometry. Utilizing these calculated fault energies within a modified Peierls-Nabarro model, we estimate the barrier for basal dislocation motion based on lattice friction. This is found to be extremely small, from which we conclude that dislocation network interaction and pinning, rather than the Peierls barrier, must determine the practical shear strength of graphite. However, at low dislocation densities or over small crystallite regions, the shear strength should tend to this lower limit. We discuss the relevance of this to the mechanism of lubrication.     

三维空间中不同视野深度位置上的返回抑制

通过虚拟现实构建虚拟三维场景,将二维平面视觉空间返回抑制范式应用到三维空间,通过两个实验操纵了目标深度、线索有效性以及视野位置三个变量,考察注意在三维空间不同视野深度位置上进行定向/重定向产生的返回抑制效应。结果发现,(1)二次线索化位于固定的中央视野时,不论目标出现在近处空间还是出现在远处空间,外周视野条件下的返回抑制大于中央视野条件下的返回抑制;(2)二次线索化位于非固定的中央视野时,近处空间和远处空间的返回抑制存在分离,表现为当目标出现在远处空间时,外周视野条件下的返回抑制效应减小。研究表明,三维空间中外周视野深度位置上的返回抑制与中央视野深度位置上的返回抑制存在差异。     

Aftereffects and the representation of stereoscopic surfaces

The structure of human disparity representation is examined through (i) adaptation experiments and (ii) model simulations of the data. Section 3 presents results of adaptation experiments designed to illuminate the structure of human disparity representation. Section 4 presents model simulations of three different disparity representation schemes. In the experiments, participants adapted to a 0.133 cycle deg-1 sinusoidally corrugated surface with 10 min of arc peak-to-trough disparity. A flat test surface was briefly presented, in which the aftereffect surface was perceived. Adapt and test surfaces were placed on disparity pedestals and thus presented in front of or behind the plane of fixation. The adapt surface could be offset from the fixation plane by +/- 8 to 24 min of arc. The test surface could be offset from the fixation plane by +/- 8 to 48 min of arc. The depth aftereffect was measured in different disparity planes by a nulling method and 'topping-up' procedure. Aftereffect tuning functions were obtained whose bandwidths, magnitudes, and tuning depended on the disparity planes of both the adapt and test surfaces. These parameters were used to constrain the models tested in section 4. On the basis of the two studies, it is argued that the human stereoscopic system encodes spatial changes of disparity using channels localised within disparity planes. A localised disparity-gradient model of the human representation of disparity is proposed.     

HRTEM study of the {252}γ austenite–martensite interface in an Fe—8Cr–1C alloy

Abstract

High-resolution transmission electron microscopy has been used to image the atomic structure of the (2S2)_γ austenite-martensite interface. By imaging along [101]_γ ∥[111]_α, the interface was viewed edge-on and seen to consist of facets on the close-packed (111)_γ, planes. From the correspondence of atoms in the close-packed planes across the austenite-martensite interface, the magnitude of the shear can be analysed as (a/24)<112> on every close-packed plane in the plane of projection. Comparison with theory indicates that this is an (a/12)<112> Burgers vector out of the plane of projection. Hence, each atomic facet can be viewed as a structural ledge containing an (a/12)<112> transformation dislocation.     

Determination of atomic structure of phason planes in the ξ′-Al–Pd–Mn phase

The atomic structures of specific types of linear defects (phason lines) and planar defects (phason planes) in the complex metallic alloy phase ξ′-Al–Pd–Mn have been determined by high-resolution electron microscopy (HREM) and theoretical HREM simulation. The results show that a representational atomic structural model for phason planes can be constructed by introducing a shift between two parts of the perfect crystalline structure using a translation vector of r ?=?(1/2) a ?+?(1/2τ) c . This typical phason plane is normally parallel to the (001) plane of the ξ′-Al–Pd–Mn phase and consists of phason lines, which are arranged side-by-side with their linear direction parallel to the [010] axis. HREM simulations, based on the structural model for both edge-on and inclined types of phason lines, agree well with the experimental results. Taking into account the fact that the structural difference between various curved phason planes arises from the variation in the arrangement of individual phason lines, the atomic structures of the edge-on and inclined phason lines can be used to explain the various curved phason planes frequently observed in the ξ′-Al–Pd–Mn phase.     

A phase-field model for deformation twinning

We propose a phase-field model for modeling microstructure evolution during deformation twinning. The order parameters are proportional to the shear strains defined in terms of twin plane orientations and twinning directions. Using a face-centered cubic Al as an example, the deformation energy as a function of shear strain is obtained using first-principle calculations. The gradient energy coefficients are fitted to the twin boundary energies along the twinning planes and to the dislocation core energies along the directions that are perpendicular to the twinning planes. The elastic strain energy of a twinned structure is included using the Khachaturyan's elastic theory. We simulated the twinning process and microstructure evolution under a number of fixed deformations and predicted the twinning plane orientations and microstructures.     

Thermal expansion coefficients of Mo-Si compounds by first-principles calculations

Taking Mo-Si compounds as model systems, we show that the coefficients of thermal expansion (CTEs) of complex structures can be calculated precisely from first principles by incorporating the Debye model for acoustic response. Specifically, we obtain a nearly isotropic CTE in MoSi₂ but a highly anisotropic CTE in Mo₅Si₃. The CTE anisotropy in Mo₅Si₃ is due to an elastically more rigid basal plane and a higher anharmonicity along the c axis. As the structure of 5-3 compounds is modified from D8_m to D8_l by boron substitutions (Mo₅SiB₂), we predict a significant decrease in the CTE anisotropy, which is confirmed by experiments.     

An investigation of lower extremity energy dissipation strategies during single-leg and double-leg landing based on sagittal and frontal plane biomechanics

There is limited understanding of the differences in lower extremity energy dissipation strategies between single-leg and double-leg landing maneuvers. This study sought to investigate these differences in sagittal and frontal planes, and explain the differences using kinematics and kinetics. We hypothesized that single-leg and double-leg landing maneuvers involve different lower extremity energy dissipation strategies in both planes. Ten recreational athletes were recruited and instructed to perform double-leg and single-leg landing from 0.60-m height. Force-plates and motion-capture system were used to obtain kinetics and kinematics data respectively. Joint power was taken as product of joint moment and angular velocity. Joint work was computed as integral of joint power over time, whereby negative work represented energy dissipation. In the sagittal plane, the hip and knee showed major contributions to energy dissipation during double-leg landing; the hip and ankle were the dominant energy dissipaters during single-leg landing. In the frontal plane, the hip acted as the key energy dissipater during double-leg landing; the knee contributed the most energy dissipation during single-leg landing. The knee also exhibited greater frontal plane joint ROM, moment and energy dissipation during single-leg landing than double-leg landing. Our findings indicated that different energy dissipation strategies were adopted for double-leg and single-leg landing in sagittal and frontal planes. Considering the prominent frontal plane biomechanics exhibited by the knee during single-leg landing, we expect that this maneuver may have greater likelihood of leading to traumatic knee injuries, particularly non-contact ACL injuries, compared to the double-leg landing maneuver.     

Spatial judgments in the horizontal and vertical planes from different vantage points

Todorovi? (2008 Perception 37 106-125) reported that there are systematic errors in the perception of 3-D space when viewing 2-D linear perspective drawings depending on the observer's vantage point. Because these findings were restricted to the horizontal plane, the current study was designed to determine the nature of these errors in the vertical plane. Participants viewed an image containing multiple colonnades aligned on parallel converging lines receding to a vanishing point. They were asked to judge where, in the physical room, the next column should be placed. The results support Todorovi? in that systematic deviations in the spatial judgments depended on vantage point for both the horizontal and vertical planes. However, there are also marked differences between the two planes. While judgments in both planes failed to compensate adequately for the vantage-point shift, the vertical plane induced greater distortions of the stimulus image itself within each vantage point.     

Surface tilt (the direction of slant): A neglected psychophysical variable

Surface slant (the angle between the line of sight and the surface normal) is an important psychophysical variable. However, slant angle captures only one of the two degrees of freedom of surface orientation, the other being thedirection of slant. Slant direction, measured in the image plane, coincides with the direction of the gradient of distance from viewer to surface and, equivalently, with the direction the surface normal would point if projected onto the image plane. Since slant direction may be quantified by the tilt of the projected normal (which ranges over 360 deg in the frontal plane), it is referred to here assurface tilt. (Note that slant angle is measured perpendicular to the image plane, whereas tilt angle is measured in the image plane.) Compared with slant angle’s popularity as a psychophysical variable, the attention paid to surface tilt seems undeservedly scant. Experiments that demonstrate a technique for measuring apparent surface tilt are reported. The experimental stimuli were oblique crosses and parallelograms, which suggest oriented planes in 3-D. The apparent tilt of the plane might be probed by orienting a needle in 3-D so as to appear normal, projecting the normal onto the image plane, and measuring its direction (e.g., relative to the horizontal). It is shown to be preferable, however, to merely rotate a line segment in 2-D, superimposed on the display, until it appears normal to the perceived surface. The apparent surface tilt recorded in these experiments corresponded closely to that predicted by assuming the 3-D configurations consist of equal-length lines and perpendicular intersections.     

TEM study of defects generated in 4H-SiC by microindentations on the prismatic plane

The deformation microstructure of single crystals of 4H-SiC resulting from microindentations on a prismatic surface was investigated by TEM. Indentations were performed at 400 and 675°C, i.e. below the brittle to ductile transition temperature of 4H-SiC (temperature close to 1100°C). TEM analysis reveals dissociated dislocations as well as extended stacking faults in the basal plane. In addition, perfect edge dislocations are observed on prismatic planes. From the observations, it is assumed that perfect dislocations are nucleated in the prismatic plane and cross-slip on the basal one where they dissociate.     

Grounding the figure: Surface attachment influences figure-ground organization

We investigated whether the lower region effect on figure-ground organization (Vecera, Vogel, & Woodman, 2002) would generalize to contextual depth planes in vertical orientations, as is predicted by a theoretical analysis based on the ecological statistics of edges arising from objects that are attached to surfaces of support. Observers viewed left/right ambiguous figure-ground displays that occluded middle sections of four types of contextual inducers: two types of attached, receding, vertical planes (walls) that used linear perspective and/or texture gradients to induce perceived depth and two types of similar trapezoidal control figures that used either uniform color or random texture to reduce or eliminate perceived depth. The results showed a reliable bias toward seeing as “figure” the side of the figure-ground display that was attached to the receding depth plane, but no such bias for the corresponding side in either of the control conditions. The results are interpreted as being consistent with the attachment hypothesis that the lower region cue to figure-ground organization results from ecological biases in edge interpretation that arise when objects are attached to supporting surfaces in the terrestrial gravitational field.     

Is the anisotropy of perceived 3-D shape invariant across scale?

A number of studies have resulted in the finding of a 3-D perceptual anisotropy, whereby spatial intervals oriented in depth are perceived to be smaller than physically equal intervals in the frontoparallel plane. In this experiment, we examined whether this anisotropy is scale invariant. The stimuli were L shapes created by two rods placed flat on a level grassy field, with one rod defining a frontoparallel interval, and the other, a depth interval. Observers monocularly and binocularly viewed L shapes at two scales such that they were projectively equivalent under monocular viewing. Observers judged the aspect ratio (depth/width) of each shape. Judged aspect ratio indicated a perceptual anisotropy that was invariant with scale for monocular viewing, but not for binocular viewing. When perspective is kept constant, monocular viewing results in perceptual anisotropy that is invariant across these two scales and presumably across still larger scales. This scale invariance indicates that the perception of shape under these conditions is determined independently of the perception of size.     

Measurement of the relative strain ratios normal to the crystal planes in Cu thin films using grazing incidence X-ray diffraction

The relative strain normal to the crystal planes in Cu thin films has been experimentally measured using grazing incidence X-ray diffraction. This was performed by measuring the ratio of the strain exerted in the same specific (hkl) crystal plane parallel and perpendicular to the film surface. The strain ratios of the (1?1?1), (2?0?0), (2?2?0) and (3?0?0) planes were found to be –0.804, –1.324, –1.003, and –1.369, respectively. These values are within experimental error of those calculated theoretically under the assumptions of plane stress conditions.